6YFG

Virus-like particle of Beihai levi-like virus 32

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	MAX IV BEAMLINE BioMAX
Synchrotron site	MAX IV
Beamline	BioMAX
Temperature [K]	100
Detector technology	PIXEL
Collection date	2018-10-19
Detector	DECTRIS EIGER X 16M
Wavelength(s)	0.97776
Spacegroup name	P 1
Unit cell lengths	291.945, 292.531, 469.196
Unit cell angles	75.79, 77.92, 69.51

Refinement procedure

Resolution	49.833 - 3.897
R-factor	0.2821
Rwork	0.282
R-free	0.28530
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	2ms2
Data reduction software	XDS
Data scaling software	XDS
Phasing software	FFT
Refinement software	PHENIX (1.14_3260)

Data quality characteristics

	Overall	Inner shell	Outer shell
Low resolution limit [Å]	49.833	49.833	4.130
High resolution limit [Å]	3.897	11.420	3.900
Rmerge	0.209	0.034	1.559
Rmeas	0.296	0.048	2.205
Number of reflections	1227552	48206	190940
<I/σ(I)>	2.97	16.98	0.38
Completeness [%]	96.2	94.9	93
Redundancy	1.8
CC(1/2)	0.985	0.997	0.151

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP	7.5	293	26% MPD, 0.1-0.2 M sodium nitrate, 0.1 M HEPES pH 7.5