6YF5
Lamin A 17-70 coil1A dimer stabilized by C-terminal capping
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-05-18 |
Detector | DECTRIS EIGER2 X 16M |
Wavelength(s) | 0.980110 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 27.374, 105.246, 119.773 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 48.220 - 1.830 |
R-factor | 0.226 |
Rwork | 0.225 |
R-free | 0.25510 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4xa3 |
RMSD bond length | 0.009 |
RMSD bond angle | 1.471 |
Data reduction software | xia2 |
Data scaling software | Aimless |
Phasing software | MOLREP |
Refinement software | REFMAC (5.8.0258) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 52.050 | 1.860 |
High resolution limit [Å] | 1.830 | 1.830 |
Number of reflections | 31710 | 1487 |
<I/σ(I)> | 9.73 | 1.08 |
Completeness [%] | 100.0 | 98.54 |
Redundancy | 10.22 | 7.6 |
CC(1/2) | 0.999 | 0.540 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 4.9 | 277 | 35.7% (w/v) 1,6-hexanediol, 5% (w/v) PEG 1K and 0.1 M trisodium citrate dihydrate |