6YDV
Crystal Structure of the Jmjc Domain of Human JMJD1B in complex with FM001511a from the DSPL fragment library
This is a non-PDB format compatible entry.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I02 |
Synchrotron site | Diamond |
Beamline | I02 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-09-30 |
Detector | DECTRIS PILATUS 2M |
Wavelength(s) | 0.9282 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 57.600, 93.790, 92.610 |
Unit cell angles | 90.00, 107.50, 90.00 |
Refinement procedure
Resolution | 54.934 - 2.070 |
Rwork | 0.170 |
R-free | 0.21370 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6rbj |
RMSD bond length | 0.004 |
RMSD bond angle | 1.309 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0258) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 54.934 | 9.260 |
High resolution limit [Å] | 2.070 | 2.070 |
Rmerge | 0.085 | 0.961 |
Rmeas | 0.130 | |
Rpim | 0.069 | 0.713 |
Number of reflections | 56778 | 4190 |
<I/σ(I)> | 10.2 | 1.3 |
Completeness [%] | 99.2 | 99.1 |
Redundancy | 3.4 | 3.5 |
CC(1/2) | 0.996 | 0.556 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5.5 | 277 | 0.1M bis-tris pH 5.5, 24% PEG3350, 0.4M magnesium chloride |