6YDF
X-ray structure of LPMO.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE MASSIF-3 |
Synchrotron site | ESRF |
Beamline | MASSIF-3 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-02-18 |
Detector | DECTRIS EIGER X 4M |
Wavelength(s) | 0.96 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 51.120, 39.390, 119.930 |
Unit cell angles | 90.00, 93.78, 90.00 |
Refinement procedure
Resolution | 50.000 - 2.120 |
R-factor | 0.19979 |
Rwork | 0.197 |
R-free | 0.24944 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5ach |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | MOLREP |
Refinement software | REFMAC (v5.8.0230) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.180 |
High resolution limit [Å] | 2.120 | 2.120 |
Number of reflections | 26050 | 1853 |
<I/σ(I)> | 8.7 | |
Completeness [%] | 94.5 | |
Redundancy | 4.02 | |
CC(1/2) | 0.995 | 0.508 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 298.15 | 0.1 M NaCl, 0.1 M HEPES pH 6.5, 1.5 M (NH4)2SO4 |