6YDD
X-ray structure of LPMO.
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE MASSIF-3 |
| Synchrotron site | ESRF |
| Beamline | MASSIF-3 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2017-04-27 |
| Detector | DECTRIS EIGER X 4M |
| Wavelength(s) | 0.90 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 52.140, 39.700, 120.650 |
| Unit cell angles | 90.00, 93.49, 90.00 |
Refinement procedure
| Resolution | 2.870 - 2.800 |
| R-factor | 0.20073 |
| Rwork | 0.198 |
| R-free | 0.26087 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 5ach |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | MOLREP |
| Refinement software | REFMAC (v5.8.0230) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 2.870 |
| High resolution limit [Å] | 2.800 | 2.800 |
| Number of reflections | 12356 | 924 |
| <I/σ(I)> | 5.82 | 1.08 |
| Completeness [%] | 98.2 | 99.1 |
| Redundancy | 5.51 | 2.96 |
| CC(1/2) | 0.969 | 0.547 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 298.15 | 0.1 M NaCl, 0.1 M Bis-Tris pH 6.5, 2.0 M (NH4)2SO4 |
