Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06SA |
| Synchrotron site | SLS |
| Beamline | X06SA |
| Temperature [K] | 93 |
| Detector technology | PIXEL |
| Collection date | 2017-12-06 |
| Detector | DECTRIS EIGER X 16M |
| Wavelength(s) | 1.00001 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 145.048, 91.614, 352.326 |
| Unit cell angles | 90.00, 92.10, 90.00 |
Refinement procedure
| Resolution | 48.068 - 2.618 |
| Rwork | 0.270 |
| R-free | 0.30030 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 4fmg |
| RMSD bond length | 0.006 |
| RMSD bond angle | 1.373 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0253) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 48.070 | 2.770 |
| High resolution limit [Å] | 2.618 | 2.618 |
| Rmeas | 0.262 | 0.156 |
| Number of reflections | 274707 | 42471 |
| <I/σ(I)> | 6.11 | 1.03 |
| Completeness [%] | 98.5 | |
| Redundancy | 3.9 | |
| CC(1/2) | 0.993 | 0.642 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 293 | HEPES, PEG 8000, ethylene glycol |
