6Y3J

RING-DTC domains of Deltex 2, bound to ADP-ribose

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	DIAMOND BEAMLINE I03
Synchrotron site	Diamond
Beamline	I03
Temperature [K]	100
Detector technology	PIXEL
Collection date	2019-02-03
Detector	DECTRIS PILATUS3 6M
Wavelength(s)	0.97625
Spacegroup name	P 32 2 1
Unit cell lengths	104.933, 104.933, 74.544
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	45.440 - 2.600
R-factor	0.2398
Rwork	0.238
R-free	0.28220
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	6y22
Data reduction software	DIALS
Data scaling software	Aimless
Phasing software	PHASER
Refinement software	PHENIX (1.17.1_3660)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	90.870	2.720
High resolution limit [Å]	2.600	2.600
Rmerge	0.270	1.618
Rpim	0.137	1.791
Number of reflections	27953	1792
<I/σ(I)>	5.3	1
Completeness [%]	100.0	100
Redundancy	9.3
CC(1/2)	0.994	0.822

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP	7.6	292	Morpheus condition 39 (Molecular Dimensions)