6XZ4
Crystal structure of TLNRD1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 1 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-11-14 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.97857 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 69.170, 58.043, 84.324 |
Unit cell angles | 90.00, 106.10, 90.00 |
Refinement procedure
Resolution | 60.218 - 2.300 |
R-factor | 0.2645 |
Rwork | 0.262 |
R-free | 0.31520 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6xz3 |
RMSD bond length | 0.004 |
RMSD bond angle | 0.792 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 60.220 | 2.380 |
High resolution limit [Å] | 2.300 | 2.300 |
Rmerge | 0.087 | 0.682 |
Rmeas | 0.108 | 0.841 |
Rpim | 0.063 | 0.487 |
Number of reflections | 28327 | 2810 |
<I/σ(I)> | 5.7 | 1.3 |
Completeness [%] | 98.4 | 98.7 |
Redundancy | 2.8 | 2.8 |
CC(1/2) | 0.994 | 0.831 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 294 | 250 mM sodium thiocyanate, 20% PEG 3350 |