6XWV
Crystal structure of drosophila melanogaster CENP-C bound to CAL1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I03 |
Synchrotron site | Diamond |
Beamline | I03 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-02-08 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.97625 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 86.273, 86.444, 88.462 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 29.080 - 2.270 |
R-factor | 0.2389 |
Rwork | 0.237 |
R-free | 0.26550 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | dmCENP-C cupin |
RMSD bond length | 0.006 |
RMSD bond angle | 1.187 |
Data reduction software | XDS (1.17.1_3660) |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (1.17.1_3660) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 29.080 | 2.350 |
High resolution limit [Å] | 2.270 | 2.270 |
Rmerge | 0.076 | 0.660 |
Number of reflections | 30957 | 2932 |
<I/σ(I)> | 21.2 | |
Completeness [%] | 98.4 | |
Redundancy | 13.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 291 | 0.2M Calcium acetate, 0.1M Na Cacodylate, pH 6.5, 18% PEG 8000 |