6XWU
Crystal structure of drosophila melanogaster CENP-C cumin domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I03 |
Synchrotron site | Diamond |
Beamline | I03 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-04-24 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.97625 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 57.195, 57.195, 92.960 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 28.600 - 1.820 |
R-factor | 0.1976 |
Rwork | 0.194 |
R-free | 0.23510 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2vpv |
RMSD bond length | 0.006 |
RMSD bond angle | 0.855 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (1.17.1_3660) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 28.600 | 1.885 |
High resolution limit [Å] | 1.820 | 1.820 |
Rmerge | 0.055 | 0.055 |
Number of reflections | 14427 | 1392 |
<I/σ(I)> | 34.13 | |
Completeness [%] | 99.7 | |
Redundancy | 18 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 291 | 50mM MES pH6.0, 45% PEG 400 |