6XWS
Crystal Structure of Drosophila CAL1 1-160 bound to CENP-A/H4
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04-1 |
Synchrotron site | Diamond |
Beamline | I04-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-04-30 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.91587 |
Spacegroup name | P 63 2 2 |
Unit cell lengths | 199.700, 199.700, 76.754 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 172.950 - 4.360 |
R-factor | 0.3072 |
Rwork | 0.306 |
R-free | 0.32290 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2pyo |
RMSD bond length | 0.004 |
RMSD bond angle | 1.175 |
Data reduction software | XDS |
Data scaling software | STARANISO |
Phasing software | PHASER |
Refinement software | PHENIX (1.17.1_3660) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 172.950 | 5.186 |
High resolution limit [Å] | 4.360 | 4.360 |
Rmerge | 0.129 | 0.950 |
Number of reflections | 2322 | 194 |
<I/σ(I)> | 9.6 | |
Completeness [%] | 89.0 | |
Redundancy | 8.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 291 | 0.2 M lithium sulfate, 0.1 M Tris pH 8.5 and 30% PEG 4000 |