6XTJ
The high resolution structure of the FERM domain of human FERMT2
This is a non-PDB format compatible entry.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I03 |
Synchrotron site | Diamond |
Beamline | I03 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-02-09 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.9763 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 145.172, 145.172, 59.633 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 72.700 - 1.600 |
Rwork | 0.181 |
R-free | 0.20370 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5xpy |
RMSD bond length | 0.008 |
RMSD bond angle | 1.428 |
Data reduction software | DIALS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0258) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 72.700 | 1.630 |
High resolution limit [Å] | 1.600 | 1.600 |
Rmerge | 0.277 | 5.732 |
Rmeas | 0.280 | 5.965 |
Rpim | 0.071 | 1.638 |
Number of reflections | 95151 | 4659 |
<I/σ(I)> | 11 | 1 |
Completeness [%] | 100.0 | 99.7 |
Redundancy | 31.1 | 25.4 |
CC(1/2) | 0.999 | 0.732 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7 | 277 | 0.1M HEPES pH 7.0, 1.4M sodium citrate tribasic |