6XSD
Patient-derived B2GPI
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-E |
Synchrotron site | APS |
Beamline | 24-ID-E |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-11-30 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.98 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 159.463, 167.566, 114.161 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 47.860 - 2.540 |
R-factor | 0.2253 |
Rwork | 0.225 |
R-free | 0.23320 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1qub |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX |
Refinement software | PHENIX (1.17.1_3660) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 2.650 |
High resolution limit [Å] | 2.540 | 5.510 | 2.560 |
Rmerge | 0.214 | 0.066 | 4.294 |
Rmeas | 0.227 | 0.070 | 4.539 |
Rpim | 0.075 | 0.023 | 1.451 |
Number of reflections | 50299 | 5249 | 4985 |
<I/σ(I)> | 6.8 | ||
Completeness [%] | 99.9 | 99.7 | 100 |
Redundancy | 8.6 | 8.4 | 9.1 |
CC(1/2) | 0.998 | 0.249 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 277 | 100mM Hepes, pH 7.5, 1.8M Ammonium Sulfate |