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6XQW

Crystal Structure of MaliM03 Fab in complex with Pfmsp1-19

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsALS BEAMLINE 5.0.2
Synchrotron siteALS
Beamline5.0.2
Temperature [K]100
Detector technologyPIXEL
Collection date2019-04-25
DetectorDECTRIS PILATUS3 6M
Wavelength(s)1.00
Spacegroup nameC 1 2 1
Unit cell lengths119.737, 69.451, 65.834
Unit cell angles90.00, 108.24, 90.00
Refinement procedure
Resolution47.016 - 2.991
R-factor0.2545
Rwork0.252
R-free0.30920
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)1ob1
RMSD bond length0.005
RMSD bond angle0.659
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Phasing softwarePHASER
Refinement softwarePHENIX (1.14_3260)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]47.0163.050
High resolution limit [Å]2.9903.000
Number of reflections10456498
<I/σ(I)>10.7
Completeness [%]99.9
Redundancy3.3
CC(1/2)0.9900.890
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP5.529320% w/v PEG 8K, 40% v/v PEG 400, 0.5M NaCl and 0.1 M acetate buffer pH 5.5

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