6XQ0
Human antibody S8V2-18 in complex with the influenza hemagglutinin head domain of A/California/7/2009(NYMC-X181)(H1N1)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-E |
Synchrotron site | APS |
Beamline | 24-ID-E |
Temperature [K] | 80 |
Detector technology | PIXEL |
Collection date | 2018-12-04 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.97918 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 160.200, 55.260, 168.000 |
Unit cell angles | 90.00, 95.02, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 44.880 | 2.383 |
High resolution limit [Å] | 2.300 | 2.300 |
Rmerge | 0.109 | 0.674 |
Rmeas | 0.134 | 0.826 |
Rpim | 0.077 | 0.471 |
Number of reflections | 62605 | 6233 |
<I/σ(I)> | 8.03 | 1.34 |
Completeness [%] | 95.2 | 96.14 |
Redundancy | 2.8 | 2.8 |
CC(1/2) | 0.991 | 0.683 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8.5 | 291.15 | 25% w/v PEG3350, 0.1 M Tris, pH 8.5 |