6XJZ
Crystal structure of a self-alkylating ribozyme - apo form
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-C |
Synchrotron site | APS |
Beamline | 24-ID-C |
Temperature [K] | 80 |
Detector technology | PIXEL |
Collection date | 2018-06-09 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.98 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 87.505, 82.419, 105.213 |
Unit cell angles | 90.00, 111.00, 90.00 |
Refinement procedure
Resolution | 81.695 - 2.488 |
R-factor | 0.2029 |
Rwork | 0.200 |
R-free | 0.26380 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6mwn |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHENIX |
Refinement software | PHENIX ((1.14_3260)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 162.730 | 2.500 |
High resolution limit [Å] | 2.460 | 2.460 |
Rmerge | 0.119 | |
Rmeas | 0.141 | 2.711 |
Rpim | 0.076 | 1.519 |
Number of reflections | 47938 | 4672 |
<I/σ(I)> | 6 | 0.5 |
Completeness [%] | 98.4 | 95.5 |
Redundancy | 3.3 | 2.8 |
CC(1/2) | 0.994 | 0.347 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.2 | 295 | 0.1 M ammonium fluoride, 10% PEG3350, pH 6.2 |