6XGZ
Crystal structure of E. coli MlaFB ABC transport subunits in the monomeric state
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 8.3.1 |
Synchrotron site | ALS |
Beamline | 8.3.1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-08-12 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 1.1158 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 78.270, 136.080, 261.830 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.870 | 2.693 |
High resolution limit [Å] | 2.600 | 2.600 |
Number of reflections | 86874 | 8606 |
<I/σ(I)> | 18.68 | |
Completeness [%] | 92.1 | |
Redundancy | 13.1 | |
CC(1/2) | 1.000 | 0.538 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5.6 | 291.15 | 0.7 M NH4H2PO4, 0.07 M Na3 Cit pH5.6, 30 %v/v Glycerol |