6XC0
Crystal structure of bacteriophage T4 spackle and lysozyme in monoclinic form
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-C |
Synchrotron site | APS |
Beamline | 24-ID-C |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-03-01 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 0.979200 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 41.310, 127.597, 46.088 |
Unit cell angles | 90.00, 92.25, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 127.430 | 1.880 |
High resolution limit [Å] | 1.780 | 1.780 |
Rmerge | 0.113 | 0.924 |
Number of reflections | 44738 | 6478 |
<I/σ(I)> | 13.1 | 1.8 |
Completeness [%] | 98.6 | |
Redundancy | 4.9 | |
CC(1/2) | 0.995 | 0.708 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 293 | 35% (w/v) polyethylene glycol 3350, 20% 2-propanol, 0.1 M HEPES-NaOH pH 7.5 |