6XA7
Crystal Structure of Human Scribble PDZ2:Vangl2 complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX1 |
Synchrotron site | Australian Synchrotron |
Beamline | MX1 |
Temperature [K] | 80 |
Detector technology | CCD |
Collection date | 2016-09-27 |
Detector | ADSC QUANTUM 210r |
Wavelength(s) | 0.9537 |
Spacegroup name | I 1 2 1 |
Unit cell lengths | 78.047, 60.765, 96.017 |
Unit cell angles | 90.00, 106.48, 90.00 |
Refinement procedure
Resolution | 47.170 - 2.500 |
R-factor | 0.2377 |
Rwork | 0.236 |
R-free | 0.26720 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | PDZ3-Vangl2 |
RMSD bond length | 0.008 |
RMSD bond angle | 0.982 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHENIX |
Refinement software | PHENIX (1.17.1_3660) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 47.174 | 2.590 |
High resolution limit [Å] | 2.500 | 2.500 |
Rmerge | 0.076 | 0.425 |
Number of reflections | 13826 | 1396 |
<I/σ(I)> | 16.2 | 4.5 |
Completeness [%] | 91.5 | 93.2 |
Redundancy | 5.7 | 5.7 |
CC(1/2) | 0.990 | 0.856 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293.15 | 0.2M Potassium thiocyanate, 20% (w/v) PEG 3350 |