6WVG
human CD53
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-E |
Synchrotron site | APS |
Beamline | 24-ID-E |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-08-19 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.9792 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 49.310, 209.770, 73.280 |
Unit cell angles | 90.00, 100.29, 90.00 |
Refinement procedure
Resolution | 35.610 - 2.900 |
R-factor | 0.2183 |
Rwork | 0.216 |
R-free | 0.26880 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2b3p |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX (1.18_3845) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 2.950 |
High resolution limit [Å] | 2.900 | 7.860 | 2.900 |
Rmerge | 0.128 | 0.027 | 0.738 |
Rmeas | 0.158 | 0.033 | 0.912 |
Rpim | 0.090 | 0.019 | 0.528 |
Total number of observations | 84126 | ||
Number of reflections | 30225 | 1508 | 1548 |
<I/σ(I)> | 6.7 | ||
Completeness [%] | 93.3 | 90.5 | 97.2 |
Redundancy | 2.8 | 2.8 | 2.8 |
CC(1/2) | 0.998 | 0.722 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | LIPIDIC CUBIC PHASE | 6 | 295 | 30% PEG 400, 0.1 M KH2PO4, 0.1 M MES pH 6.0 |