6WRO
CRYSTAL STRUCTURE OF INOSITOL POLYPHOSPHATE 1-PHOSPHATASE INPP1 IN COMPLEX GADOLINIUM BUT NO LITHIUM AT 3 ANGSTROM RESOLUTION
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Temperature [K] | 296 |
Detector technology | AREA DETECTOR |
Collection date | 1994-08-10 |
Detector | UCSD MARK II |
Wavelength(s) | 1.542 |
Spacegroup name | P 41 |
Unit cell lengths | 51.640, 51.640, 143.330 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 8.280 - 3.000 |
R-factor | 0.19534 |
Rwork | 0.193 |
R-free | 0.23590 |
Structure solution method | FOURIER SYNTHESIS |
Starting model (for MR) | 1inp |
RMSD bond length | 0.006 |
RMSD bond angle | 0.817 |
Data reduction software | UCSD-system |
Data scaling software | UCSD-system |
Phasing software | SQUASH |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 8.300 | 3.230 |
High resolution limit [Å] | 3.000 | 3.000 |
Number of reflections | 12719 | 1000 |
<I/σ(I)> | 3.5 | |
Completeness [%] | 78.6 | 70 |
Redundancy | 1.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.25 | 293 | 10% PEG 8000, 80mM Bis-Tris, pH 5.25, 2mM Gd2(SO4)3 |