6WLG
Ints3 C-terminal Domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-C |
Synchrotron site | APS |
Beamline | 24-ID-C |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-06-15 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.979 |
Spacegroup name | H 3 |
Unit cell lengths | 234.854, 234.854, 47.567 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 46.317 - 3.111 |
R-factor | 0.2065 |
Rwork | 0.204 |
R-free | 0.26330 |
Structure solution method | SAD |
RMSD bond length | 0.003 |
RMSD bond angle | 0.777 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | SHELXCD |
Refinement software | PHENIX (1.15.2_3472) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 46.320 | 3.330 |
High resolution limit [Å] | 3.110 | 3.110 |
Rmerge | 0.060 | 0.570 |
Number of reflections | 17495 | 3181 |
<I/σ(I)> | 14.6 | 2.5 |
Completeness [%] | 99.5 | |
Redundancy | 5.3 | |
CC(1/2) | 0.998 | 0.896 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 289 | 0.2 M Magnesium Acetate, 13% PEG 3350 |