6WJE
Copper resistance protein copG- Form 2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-E |
Synchrotron site | APS |
Beamline | 24-ID-E |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-12-08 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.9792 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 63.700, 87.460, 143.270 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 55.420 - 2.500 |
R-factor | 0.1938 |
Rwork | 0.188 |
R-free | 0.24540 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6wis |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX (dev_3724) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 55.420 | 2.570 |
High resolution limit [Å] | 2.500 | 2.500 |
Rmeas | 0.148 | |
Number of reflections | 28435 | 2067 |
<I/σ(I)> | 8.93 | 1.9 |
Completeness [%] | 99.8 | |
Redundancy | 6.62 | |
CC(1/2) | 0.996 | 0.566 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.8 | 298 | 100 mM Na Cacodylate pH 6.8 200 mM Zn Acetate 19% ethanol |