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6W3T

Crystal structure of ligand-binding domain of Campylobacter jejuni chemoreceptor Tlp3 in complex with L-norvaline

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsAUSTRALIAN SYNCHROTRON BEAMLINE MX1
Synchrotron siteAustralian Synchrotron
BeamlineMX1
Temperature [K]100
Detector technologyCCD
Collection date2016-11-10
DetectorADSC QUANTUM 210r
Wavelength(s)0.9537
Spacegroup nameP 1 21 1
Unit cell lengths41.931, 137.770, 49.190
Unit cell angles90.00, 93.92, 90.00
Refinement procedure
Resolution39.969 - 2.100
R-factor0.1613
Rwork0.159
R-free0.20420
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)4xmr
RMSD bond length0.006
RMSD bond angle0.794
Data reduction softwareiMOSFLM
Data scaling softwareAimless
Phasing softwarePHASER
Refinement softwarePHENIX (1.10.1_2155)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]46.2302.160
High resolution limit [Å]2.1002.100
Rmerge0.077
Rmeas0.313
Number of reflections31594
<I/σ(I)>10.6
Completeness [%]97.6
Redundancy4.3
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP298PEG 3350, sodium citrate and ammonium sulphate

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