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6VZF

Crystal Structure of Atg11 Coiled-Coil 3

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsAPS BEAMLINE 24-ID-C
Synchrotron siteAPS
Beamline24-ID-C
Temperature [K]80
Detector technologyPIXEL
Collection date2018-11-02
DetectorDECTRIS PILATUS3 6M
Wavelength(s)0.979100
Spacegroup nameP 31 2 1
Unit cell lengths103.105, 103.105, 37.520
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution34.610 - 2.030
R-factor0.2273
Rwork0.226
R-free0.24590
Structure solution methodSAD
RMSD bond length0.012
RMSD bond angle1.719
Data reduction softwareXDS
Data scaling softwareAimless (0.7.3)
Phasing softwareAutoSol
Refinement softwareREFMAC (5.8.0258)
Data quality characteristics
 OverallInner shellOuter shell
Low resolution limit [Å]44.65044.6502.080
High resolution limit [Å]2.0309.0802.030
Rmerge0.1070.0591.852
Rmeas0.1090.0601.901
Rpim0.0240.0140.427
Total number of observations303942329221698
Number of reflections150631891110
<I/σ(I)>16.757.62
Completeness [%]99.997.7100
Redundancy20.217.419.5
CC(1/2)0.9990.9990.661
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP29590 mM LiNaK, 0.1 M Buffer system 4 pH 6.5 (MOPSO + Bis Tris), 50% v/v precipitant mix 6 (25% w/v PEG 4000, 40% w/v 1,2,6-hexanetriol)
1VAPOR DIFFUSION, HANGING DROP29590 mM LiNaK, 0.1 M Buffer system 4 pH 6.5 (MOPSO + Bis Tris), 50% v/v precipitant mix 6 (25% w/v PEG 4000, 40% w/v 1,2,6-hexanetriol)

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PDB entries from 2024-07-17

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