6VVR
Q0 fused 4-OT wild type symmetric trimer
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 5.0.1 |
Synchrotron site | ALS |
Beamline | 5.0.1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-04-20 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 1.0332 |
Spacegroup name | P 43 |
Unit cell lengths | 72.943, 72.943, 82.299 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 35.840 - 1.800 |
Rwork | 0.172 |
R-free | 0.20540 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5unq |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | MOLREP |
Refinement software | PHENIX (v1.16) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 35.840 | 1.860 |
High resolution limit [Å] | 1.800 | 1.800 |
Number of reflections | 39332 | 3844 |
<I/σ(I)> | 11.5 | |
Completeness [%] | 98.8 | 96.6 |
Redundancy | 5.6 | |
CC(1/2) | 0.996 | 0.738 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 298.15 | 0.2 M ammonium sulfate, 27-33% PEG4000 |