6VVM
R7 fused 4-OT wild type asymmetric trimer
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 23-ID-D |
Synchrotron site | APS |
Beamline | 23-ID-D |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-03-03 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 1.0332 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 149.714, 49.957, 48.028 |
Unit cell angles | 90.00, 100.54, 90.00 |
Refinement procedure
Resolution | 47.220 - 1.830 |
Rwork | 0.187 |
R-free | 0.22850 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6blm |
RMSD bond length | 0.009 |
RMSD bond angle | 0.937 |
Data reduction software | HKL-2000 (1) |
Data scaling software | HKL-2000 (1) |
Phasing software | MOLREP (1) |
Refinement software | PHENIX (1.16.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 47.220 | 1.900 |
High resolution limit [Å] | 1.830 | 1.830 |
Rmerge | 0.131 | |
Rpim | 0.078 | |
Number of reflections | 29709 | 2277 |
<I/σ(I)> | 8.2 | |
Completeness [%] | 97.1 | 76 |
Redundancy | 3.5 | |
CC(1/2) | 0.988 | 0.790 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.2 M ammonium sulfate, 15-30% PEG5000 MME |