6VN5
USP7 IN COMPLEX WITH LIGAND COMPOUND 7
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-07-01 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 1.0 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 70.430, 65.078, 85.189 |
Unit cell angles | 90.00, 93.58, 90.00 |
Refinement procedure
Resolution | 47.800 - 2.900 |
R-factor | 0.2157 |
Rwork | 0.213 |
R-free | 0.26780 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 1.103 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | MOLREP |
Refinement software | REFMAC (5.8.0049) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 85.020 | 3.150 |
High resolution limit [Å] | 2.900 | 2.900 |
Rmerge | 0.064 | 0.443 |
Rmeas | 0.074 | 0.034 |
Number of reflections | 17172 | 3727 |
<I/σ(I)> | 15.68 | 3.55 |
Completeness [%] | 99.3 | 98.9 |
Redundancy | 4 | 3.8 |
CC(1/2) | 0.998 | 0.906 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 277 |