6VN4
USP7 IN COMPLEX WITH LIGAND COMPOUND 1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-05-14 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9999 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 75.380, 70.715, 78.551 |
Unit cell angles | 90.00, 93.40, 90.00 |
Refinement procedure
Resolution | 44.000 - 2.690 |
R-factor | 0.2443 |
Rwork | 0.242 |
R-free | 0.29990 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | In House Model |
RMSD bond length | 0.015 |
RMSD bond angle | 1.731 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0135) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 78.410 | 2.940 |
High resolution limit [Å] | 2.690 | 2.690 |
Rmerge | 0.037 | 0.449 |
Rmeas | 0.045 | 0.550 |
Number of reflections | 21844 | 87 |
<I/σ(I)> | 12.86 | 2.72 |
Completeness [%] | 94.4 | 98.1 |
Redundancy | 3 | 3 |
CC(1/2) | 0.999 | 0.937 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 277 | NULL |