6VKF

CCHFV GP38 (IbAr10200)

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 19-ID
Synchrotron site	APS
Beamline	19-ID
Temperature [K]	100
Detector technology	CCD
Collection date	2018-11-09
Detector	ADSC QUANTUM 315
Wavelength(s)	0.979
Spacegroup name	P 1 21 1
Unit cell lengths	62.350, 97.870, 66.010
Unit cell angles	90.00, 103.87, 90.00

Refinement procedure

Resolution	51.481 - 2.524
R-factor	0.2243
Rwork	0.223
R-free	0.25580
Structure solution method	SAD
Data reduction software	MOSFLM
Data scaling software	Aimless
Phasing software	PHASER
Refinement software	PHENIX (1.14_3260)

Data quality characteristics

	Overall	Inner shell	Outer shell
Low resolution limit [Å]	51.481	2.940	2.630
High resolution limit [Å]	2.520	2.790	2.520
Number of reflections	25110	2584	2868
<I/σ(I)>	12.6	1.5	2.5
Completeness [%]	97.0
Redundancy	3.2
CC(1/2)	0.998	0.733	0.815

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		293	Sodium acetate pH 5.5, PEG 400, PEG 3350
1	VAPOR DIFFUSION, HANGING DROP		293	Sodium acetate pH 5.5, PEG 400, PEG 3350