6VKF
CCHFV GP38 (IbAr10200)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 19-ID |
Synchrotron site | APS |
Beamline | 19-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2018-11-09 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.979 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 62.350, 97.870, 66.010 |
Unit cell angles | 90.00, 103.87, 90.00 |
Refinement procedure
Resolution | 51.481 - 2.524 |
R-factor | 0.2243 |
Rwork | 0.223 |
R-free | 0.25580 |
Structure solution method | SAD |
Data reduction software | MOSFLM |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (1.14_3260) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 51.481 | 2.940 | 2.630 |
High resolution limit [Å] | 2.520 | 2.790 | 2.520 |
Number of reflections | 25110 | 2584 | 2868 |
<I/σ(I)> | 12.6 | 1.5 | 2.5 |
Completeness [%] | 97.0 | ||
Redundancy | 3.2 | ||
CC(1/2) | 0.998 | 0.733 | 0.815 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | Sodium acetate pH 5.5, PEG 400, PEG 3350 | |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | Sodium acetate pH 5.5, PEG 400, PEG 3350 |