6VJO
Human parainfluenza virus type 3 fusion glycoprotein N-terminal heptad repeat domain+alpha/beta-VI
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | BRUKER AXS MICROSTAR |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2016-07-01 |
Detector | BRUKER SMART 6000 |
Wavelength(s) | 1.542 |
Spacegroup name | H 3 |
Unit cell lengths | 48.345, 48.345, 134.546 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 35.550 - 2.000 |
R-factor | 0.2021 |
Rwork | 0.200 |
R-free | 0.22560 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1ztm |
RMSD bond length | 0.005 |
RMSD bond angle | 0.745 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX (1.17.1_3660) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 35.550 | 2.130 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmeas | 0.171 | 0.944 |
Rpim | 0.058 | 0.478 |
Number of reflections | 7675 | 1107 |
<I/σ(I)> | 10.5 | 2.4 |
Completeness [%] | 96.8 | 83.9 |
Redundancy | 8.7 | |
CC(1/2) | 0.996 | 0.426 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 298 | 30 mM NaF, 30 mM NaBr, 30 mM NaI, 20% (v/v) PEG 500 MME, 10% (w/v) PEG 20000 in 100 mM imidazole/MES monohydrate buffer (pH 6.5) |