6VIT
The Crystal Structure of Apo Domain-Swapped dimer Q108K:T51D:I32C Variant of HCRBPII with an Engineered Disulfide Bond
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 21-ID-D |
Synchrotron site | APS |
Beamline | 21-ID-D |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-11-17 |
Detector | DECTRIS EIGER2 X 9M |
Wavelength(s) | 0.97624 |
Spacegroup name | P 63 |
Unit cell lengths | 133.283, 133.283, 51.160 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 38.480 - 3.200 |
R-factor | 0.2388 |
Rwork | 0.233 |
R-free | 0.28770 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2rct |
RMSD bond length | 0.009 |
RMSD bond angle | 1.177 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX (1.14_3260) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 3.420 |
High resolution limit [Å] | 3.200 | 3.200 |
Rmerge | 0.200 | 1.100 |
Rmeas | 0.210 | |
Number of reflections | 8637 | 843 |
<I/σ(I)> | 13.85 | 2.1 |
Completeness [%] | 99.4 | |
Redundancy | 5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.4 | 298 | citric acid, PEG 3350 |