6VIK
Crystal structure of mouse xm RABL3 in complex with GTPgammsS
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 19-ID |
Synchrotron site | APS |
Beamline | 19-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2019-10-17 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.979 |
Spacegroup name | P 65 2 2 |
Unit cell lengths | 61.117, 61.117, 224.311 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 47.866 - 1.700 |
R-factor | 0.2094 |
Rwork | 0.207 |
R-free | 0.23480 |
Structure solution method | SAD |
Data reduction software | HKL-3000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX (1.15.2_3472) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 1.730 |
High resolution limit [Å] | 1.700 | 4.610 | 1.700 |
Rmerge | 0.126 | 0.041 | 5.362 |
Rmeas | 0.128 | 0.041 | 5.483 |
Rpim | 0.022 | 0.007 | 1.130 |
Total number of observations | 960436 | ||
Number of reflections | 28484 | 1665 | 1357 |
<I/σ(I)> | 6.3 | ||
Completeness [%] | 100.0 | 99.7 | 99.9 |
Redundancy | 33.7 | 31.9 | 23.4 |
CC(1/2) | 0.998 | 0.568 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 277 | 0.1 M Sodium citrate tribasic dihydrate pH 5.0, 16% EG 1000 |