6VID
The Crystal Structure of Aps Domain-Swapped Trimer Q108K:K40D:T53A:R58L:Q38F:Q4F Variant of HCRBPII
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 21-ID-F |
Synchrotron site | APS |
Beamline | 21-ID-F |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2017-02-21 |
Detector | RAYONIX MX-300 |
Wavelength(s) | 0.97872 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 67.050, 72.680, 164.798 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 49.280 - 2.890 |
R-factor | 0.2515 |
Rwork | 0.245 |
R-free | 0.30780 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2rcq |
RMSD bond length | 0.005 |
RMSD bond angle | 0.920 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX |
Refinement software | PHENIX (1.14_3260) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.282 | 2.994 |
High resolution limit [Å] | 2.891 | 2.891 |
Rmerge | 0.170 | 0.115 |
Rmeas | 0.178 | 1.316 |
Rpim | 0.047 | |
Number of reflections | 18585 | 1745 |
<I/σ(I)> | 2.4 | |
Completeness [%] | 99.4 | |
Redundancy | 7.7 | |
CC(1/2) | 0.804 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 298 | PEG 4000, Sodium acetate, Ammonium acetate |