6VD8
Metal-bound C-terminal domain of CzcD transporter from Pseudomonas aeruginosa
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
Synchrotron site | Australian Synchrotron |
Beamline | MX2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-06-01 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 1.2652 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 36.916, 58.247, 72.014 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 45.290 - 2.300 |
R-factor | 0.24102 |
Rwork | 0.238 |
R-free | 0.27137 |
Structure solution method | SAD |
RMSD bond length | 0.002 |
RMSD bond angle | 1.154 |
Data reduction software | XDS (5.8.0238) |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | REFMAC (7.0.073) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 45.290 | 2.370 |
High resolution limit [Å] | 2.290 | 2.290 |
Number of reflections | 7349 | 653 |
<I/σ(I)> | 10.2 | |
Completeness [%] | 99.3 | |
Redundancy | 25.6 | |
CC(1/2) | 0.998 | 0.881 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 0.2 M ammonium acetate, 0.1 M Bis-Tris pH 7.2, 30% (w/v) PEG 3350, 1.0 mM ZnCl2 |