6VCP
Crystal structure of E.coli RppH in complex with UTP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2013-09-19 |
Detector | RIGAKU RAXIS IV++ |
Wavelength(s) | 1.5418 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 78.783, 38.739, 58.757 |
Unit cell angles | 90.00, 101.01, 90.00 |
Refinement procedure
Resolution | 19.370 - 1.700 |
R-factor | 0.1831 |
Rwork | 0.182 |
R-free | 0.20830 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4s2y |
RMSD bond length | 0.011 |
RMSD bond angle | 1.209 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHENIX |
Refinement software | PHENIX (1.16_3546) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 19.370 | 1.760 |
High resolution limit [Å] | 1.700 | 1.700 |
Number of reflections | 19245 | 1896 |
<I/σ(I)> | 15.6 | |
Completeness [%] | 99.2 | |
Redundancy | 3.9 | |
CC(1/2) | 0.990 | 0.770 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293.15 | 0.4 M (NH4)2SO4, 10% (v/v) PEG3350, 10% (v/v) glycerol |