6VC1

Octreotide oxalate

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SLS BEAMLINE X04SA
Temperature [K]	293
Detector technology	PIXEL
Collection date	2018-09-12
Detector	MYTHEN II Silicon Solid State 1D detector system
Wavelength(s)	1.3004392
Spacegroup name	P 21 21 21
Unit cell lengths	18.529, 30.288, 39.731
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	? - ?
Refinement software	GSAS

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	EVAPORATION, RECRYSTALLIZATION		298	0.2 M oxalic acid 434 mg mL-1 octreotide acetate 322.8 K until almost complete evaporation Redesolution in ddH2O 298 K until almost complete evaporation Repeat until crystal formation