6V96
Agrobacterium tumefaciens ADP-Glucose pyrophosphorylase-S72E
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 21-ID-F |
Synchrotron site | APS |
Beamline | 21-ID-F |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2018-02-06 |
Detector | RAYONIX MX300HE |
Wavelength(s) | 0.978 |
Spacegroup name | P 1 |
Unit cell lengths | 93.607, 141.187, 229.427 |
Unit cell angles | 107.93, 101.72, 89.97 |
Refinement procedure
Resolution | 37.390 - 1.800 |
R-factor | 0.195 |
Rwork | 0.193 |
R-free | 0.22760 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5w6j |
RMSD bond length | 0.011 |
RMSD bond angle | 1.089 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | PHENIX (1.11.1_2575) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 37.400 | 1.830 |
High resolution limit [Å] | 1.790 | 1.790 |
Rmeas | 0.060 | |
Rpim | 0.042 | |
Number of reflections | 776640 | 41416 |
<I/σ(I)> | 1 | |
Completeness [%] | 82.0 | |
Redundancy | 1.5 | |
CC(1/2) | 0.604 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 297 | Sodium citrate, imidazole |