6V8M
Crystal structure of Ara h 8.0201
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 22-ID |
Synchrotron site | APS |
Beamline | 22-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2015-02-22 |
Detector | RAYONIX MX300-HS |
Wavelength(s) | 1.0000 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 118.668, 42.012, 81.936 |
Unit cell angles | 90.00, 124.25, 90.00 |
Refinement procedure
Resolution | 30.760 - 1.750 |
R-factor | 0.1846 |
Rwork | 0.183 |
R-free | 0.21900 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6v8j |
RMSD bond length | 0.009 |
RMSD bond angle | 1.509 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | MOLREP |
Refinement software | REFMAC (5.8.0257) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.000 | 1.780 |
High resolution limit [Å] | 1.750 | 1.750 |
Rmerge | 0.054 | 0.566 |
Rmeas | 0.062 | 0.655 |
Rpim | 0.031 | 0.324 |
Number of reflections | 33202 | 1656 |
<I/σ(I)> | 34 | 2.4 |
Completeness [%] | 98.0 | 100 |
Redundancy | 4.1 | 4.1 |
CC(1/2) | 0.869 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 8 | 298 | 0.1M HEPES, 2.0M Ammonium Sulfate, pH 8.0 |