6V6M
Crystal structure of an inactive state of GMPPNP-bound RhoA
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 31-ID |
Synchrotron site | APS |
Beamline | 31-ID |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-08-10 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.97931 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 32.267, 86.836, 34.040 |
Unit cell angles | 90.00, 96.18, 90.00 |
Refinement procedure
Resolution | 33.840 - 1.390 |
R-factor | 0.2139 |
Rwork | 0.213 |
R-free | 0.23590 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1kmq |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX (1.17.1_3660) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 86.840 | 1.460 |
High resolution limit [Å] | 1.390 | 1.390 |
Rmerge | 0.070 | 0.530 |
Rmeas | 0.095 | 0.715 |
Number of reflections | 37096 | 5469 |
<I/σ(I)> | 10.2 | 2.1 |
Completeness [%] | 98.9 | |
Redundancy | 3.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8.3 | 277 | 20-24% PEG8K, 15% Dioxane, 0.1M Tris pH8.0 |