6V5I
Coiled-coil Trimer with Ala:Leu:Ala Triad
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | ENRAF-NONIUS FR591 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2017-08-18 |
Detector | APEX II CCD |
Wavelength(s) | 1.5406 |
Spacegroup name | H 3 |
Unit cell lengths | 37.860, 37.860, 105.847 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 31.310 - 1.900 |
R-factor | 0.1593 |
Rwork | 0.155 |
R-free | 0.19300 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5uxt |
Data reduction software | PROTEUM PLUS |
Data scaling software | PROTEUM PLUS |
Phasing software | PHENIX |
Refinement software | PHENIX (dev_2906) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 31.320 | 2.046 |
High resolution limit [Å] | 1.900 | 1.900 |
Rmerge | 0.138 | 0.347 |
Number of reflections | 4461 | 1119 |
<I/σ(I)> | 7.7 | 1.1 |
Completeness [%] | 99.2 | |
Redundancy | 3.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 298 | 40% PEG300, 100 mM HEPES/NaOH, pH 7.5, 200 mM sodium chloride |