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6V4C

Culex quinquefasciatus D7 long form 1- CxD7L1 in complex with ADP

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsAPS BEAMLINE 22-BM
Synchrotron siteAPS
Beamline22-BM
Temperature [K]95
Detector technologyCCD
Collection date2019-10-19
DetectorRAYONIX MX300-HS
Wavelength(s)1.0000
Spacegroup nameI 21 21 21
Unit cell lengths76.660, 84.320, 132.070
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution39.020 - 1.970
R-factor0.2151
Rwork0.214
R-free0.23490
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)3nht
Data reduction softwareXDS
Data scaling softwareXSCALE
Phasing softwarePHASER
Refinement softwarePHENIX (1.17.1_3660)
Data quality characteristics
 OverallInner shellOuter shell
Low resolution limit [Å]39.02039.0202.020
High resolution limit [Å]1.9708.8101.970
Rmerge0.0660.0380.643
Rmeas0.0720.0420.705
Total number of observations179520
Number of reflections303643322235
<I/σ(I)>12.1919.712.35
Completeness [%]99.183.6100
Redundancy5.91255.948
CC(1/2)0.9980.9980.839
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP6.52930.1 M MES monohydrate, pH 6.5, 25% 550 PEG MME, 0.01 M Zn sulfate

227561

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