6UYX
Crystal structure of K37-acetylated SUMO1 in complex with phosphorylated DAXX
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | CHESS BEAMLINE F1 |
Synchrotron site | CHESS |
Beamline | F1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-05-28 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 0.97750 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 34.292, 81.452, 34.284 |
Unit cell angles | 90.00, 112.41, 90.00 |
Refinement procedure
Resolution | 31.690 - 1.700 |
R-factor | 0.169 |
Rwork | 0.159 |
R-free | 0.21000 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4wjn |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX (1.14-3260_1496) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 31.694 | 1.761 |
High resolution limit [Å] | 1.700 | 1.700 |
Number of reflections | 18373 | 1554 |
<I/σ(I)> | 8.6 | |
Completeness [%] | 95.8 | |
Redundancy | 3.3 | |
CC(1/2) | 0.996 | 0.269 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 298 | 100MM SODIUM CACODYLATE PH6.5, 26% PEG3350, 10MM CALCIUM CHLORIDE |