6UYU
Crystal structure of K45-acetylated SUMO1 in complex with phosphorylated PML-SIM
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | CLSI BEAMLINE 08ID-1 |
Synchrotron site | CLSI |
Beamline | 08ID-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-06-13 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 0.9795 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 38.536, 63.136, 91.378 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 37.010 - 1.660 |
R-factor | 0.171 |
Rwork | 0.169 |
R-free | 0.18600 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4wjn |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX (1.14-3260_1496) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 37.014 | 1.717 |
High resolution limit [Å] | 1.658 | 1.658 |
Number of reflections | 25859 | 1821 |
<I/σ(I)> | 12.68 | |
Completeness [%] | 95.1 | |
Redundancy | 6.2 | |
CC(1/2) | 0.999 | 0.999 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 298 | 100MM SODIUM CACODYLATE PH6.5, 16% PEG3350, 10MM CALCIUM CHLORIDE |