6UYR
Crystal structure of K46-acetylated SUMO1 in complex with PML-SIM
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | CLSI BEAMLINE 08ID-1 |
Synchrotron site | CLSI |
Beamline | 08ID-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-07-29 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 0.9795 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 38.373, 47.070, 63.179 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 32.797 - 1.300 |
R-factor | 0.1574 |
Rwork | 0.156 |
R-free | 0.17330 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4wjo |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX (1.14-3260_1496) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 32.797 | 1.347 |
High resolution limit [Å] | 1.300 | 1.300 |
Number of reflections | 28366 | 2449 |
<I/σ(I)> | 16.26 | |
Completeness [%] | 98.4 | 85.27 |
Redundancy | 6 | |
CC(1/2) | 0.999 | 0.392 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 298 | 100MM SODIUM CACODYLATE PH6.5, 16% PEG3350, 10MM CALCIUM CHLORIDE |