6USW
CRYSTAL STRUCTURE OF HIV-1 LM/HS CLADE A/E CRF01 GP120 CORE IN COMPLEX WITH (S)-MCG-IV-210
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL12-2 |
Synchrotron site | SSRL |
Beamline | BL12-2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-05-20 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.97946 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 65.817, 66.585, 86.151 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 33.292 - 2.500 |
R-factor | 0.2488 |
Rwork | 0.246 |
R-free | 0.30060 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3tgt |
RMSD bond length | 0.007 |
RMSD bond angle | 0.951 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX ((1.15.2_3472: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.540 |
High resolution limit [Å] | 2.500 | 2.500 |
Rmerge | 0.118 | |
Rpim | 0.060 | 0.600 |
Number of reflections | 10448 | 563 |
<I/σ(I)> | 14.5 | 0.8 |
Completeness [%] | 76.5 | 81.2 |
Redundancy | 3.7 | 3.5 |
CC(1/2) | 0.970 | 0.590 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 298 | 10% PEG 3350, 5% PEG 400, 0.1 M HEPES pH 7.5 |