6UOQ
OsPYL/RCAR5 residues 24-29 solved from electron diffraction stills
Experimental procedure
Source type | ELECTRON MICROSCOPE |
Source details | TEAM1 |
Temperature [K] | 100 |
Detector technology | CMOS CAMERA |
Collection date | 2019-04-04 |
Detector | K2 IS |
Wavelength(s) | 0.0197 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 4.720, 11.560, 39.190 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 7.474 - 1.007 |
R-factor | 0.2358 |
Rwork | 0.234 |
R-free | 0.25570 |
Data scaling software | XSCALE |
Refinement software | PHENIX |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 7.474 | 7.474 | 1.200 |
High resolution limit [Å] | 1.000 | 8.000 | 1.000 |
Rmerge | 0.217 | 0.357 | |
Rmeas | 0.266 | 0.440 | |
Total number of observations | 2878 | ||
Number of reflections | 1029 | 400 | |
<I/σ(I)> | 2.87 | 1.8 | |
Completeness [%] | 74.4 | 70.9 | |
Redundancy | 2.797 | 2.685 | |
CC(1/2) | 0.955 | 0.941 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 298 | 10% ethanol |