6UF1
Pistol ribozyme transition-state analog vanadate
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-C |
Synchrotron site | APS |
Beamline | 24-ID-C |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-02-21 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 1.89170 |
Spacegroup name | P 42 21 2 |
Unit cell lengths | 90.570, 90.570, 122.558 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 19.981 - 3.100 |
R-factor | 0.2048 |
Rwork | 0.199 |
R-free | 0.25470 |
Structure solution method | MOLECULAR REPLACEMENT |
Data reduction software | MOSFLM |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (1.15.2_3472) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 122.600 | 3.080 |
High resolution limit [Å] | 2.900 | 2.900 |
Rpim | 0.046 | 5.326 |
Number of reflections | 10544 | |
<I/σ(I)> | 11.2 | |
Completeness [%] | 98.9 | |
Redundancy | 8.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 293 | 0.05 M HEPES sodium, pH 7.5, 0.1 M manganese chloride, 25% MPD |