6U9J

Crystal structure of ChuX

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 22-ID
Synchrotron site	APS
Beamline	22-ID
Temperature [K]	291
Detector technology	PIXEL
Collection date	2018-02-11
Detector	DECTRIS EIGER X 16M
Wavelength(s)	0.98
Spacegroup name	P 32
Unit cell lengths	50.566, 50.566, 208.969
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	33.560 - 1.500
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	2ovi
Data reduction software	HKL-3000
Data scaling software	HKL-3000
Phasing software	PHENIX
Refinement software	PHENIX ((1.12_2829: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	1.550
High resolution limit [Å]	1.500	1.500
Number of reflections	95633	8000
<I/σ(I)>	36.6
Completeness [%]	97.3
Redundancy	13.3
CC(1/2)	0.999	0.995

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	COUNTER-DIFFUSION		293	0.2 M lithium sulfate monohydrate, 20% w/v PEG3350