6U7B
Structure of E. coli MS115-1 CdnC:HORMA-deltaN complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-C |
Synchrotron site | APS |
Beamline | 24-ID-C |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-07-11 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.9791 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 52.286, 142.897, 151.157 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 103.840 - 2.090 |
R-factor | 0.2065 |
Rwork | 0.205 |
R-free | 0.23300 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6p80 |
RMSD bond length | 0.003 |
RMSD bond angle | 0.628 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (1.16_3549) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 151.160 | 2.140 |
High resolution limit [Å] | 2.090 | 2.090 |
Rmerge | 0.081 | 1.305 |
Rmeas | 0.089 | 1.414 |
Rpim | 0.034 | 0.537 |
Number of reflections | 67360 | 4202 |
<I/σ(I)> | 16.2 | 1.4 |
Completeness [%] | 99.5 | 94.1 |
Redundancy | 6.6 | 6.6 |
CC(1/2) | 0.999 | 0.566 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 0.1 M CHES pH 9.5, 0.1 M magnesium acetate, and 17% PEG 3350 |